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High-Temperature Size Exclusion Chromatography (HT-SEC)

Laboratory

Professor Denis Rodrigue’s Laboratory


Department

Department of Chemical Engineering


Funding agency(ies)

Conseil de recherches en sciences naturelles et en génie du Canada (CRSNG)


Manufacturer (model)

Viscotek/Malvern (HT-GPC module 350)


Equipment Description

Size exclusion chromatography (SEC) is an analytical technique used to characterize polymers in solution. This technique is also known as gel permeation chromatography (GPC). It enables the determination of the number-average molar mass (Mn), weight-average molar mass (Mw), and polydispersity index (PDI) of materials. In an SEC or GPC column, polymer chains are separated according to their hydrodynamic diameter. This particular instrument allows the analysis of polymers that can only be dissolved at elevated temperatures. It also enables viscosity measurements.


Technical Specifications

  • Mobile phase: Organic solvents only

  • Maximum temperature: 160 °C

  • Four detectors: Refractive index, UV–Vis, light scattering, and viscometer

  • Detection mode: Single or multi-detection (2 or 3 simultaneous detectors)

  • Automated sample injector


Areas of expertise

  • Materials science

  • Nanoscience and nanotechnology

  • Polymers


Conditions of Use

Training on the instrument is required, or the instrument must be operated by a research professional. Available to academic and/or industrial collaborators.


Rental Fees (CAD)


On-Campus

200$/ sample


Off-Campus (Academic)

200$/ sample


Industry

300$/ sample


Reservations

Denis Rodrigue

denis.rodrigue@gch.ulaval.ca



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